Metallpulver med hög renhet

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Översikt av metallpulver med hög renhet

High purity metal powders refer to metals processed into fine particulate form while minimizing contamination from oxygen, nitrogen, carbon, and other elements. Maintaining ultra-low impurity levels allows manufacturing of products like electronic conductors, magnetic materials, superalloys, and welding wires with tightly controlled chemistry.

Applications range from 3D printing to electronics to aerospace components. Typical high purity metals include nickel, cobalt, copper, aluminum alloys, as well as refractory metals like tungsten, molybdenum, and tantalum. Both elemental metals and master alloys with addition of alloying elements are covered at purity levels exceeding 99%.

High Purity Metal Powder Types

MaterialRenhetsnivåerProduktionsmetoderEgenskaperTillämpningar
NickelUp to 99.998%KarbonylprocessExcellent conductivity, magneticsElectronics, batteries
KopparUpp till 99,999%ElektrolysHigh electric and thermal conductivityWelding wires, electronics
KoboltUp to 99.95%HydrometallurgyBibehåller styrkan vid höga temperaturerCutting tools, magnets
VolframUpp till 99,99%Hydrogen reductionVery high density, strengthLight bulb filaments, counterweights
TantalumUp to 99.997%Smältning med elektronstråleUtmärkt korrosionsbeständighetCapacitors, medical implants
AluminiumlegeringarUpp till 99,99%AtomiseringLättvikt, hög hållfasthetAerospace components, automotive
metallpulver med hög renhet

metallpulver med hög renhet Produktionsmetoder

Key techniques for producing pure metal powders include:

  • Elektrolys: Used for Cu, Zn, Ni. Electroplating deposits pure metal onto cathodes which is scraped off as powder.
  • Karbonylprocessen: Used for Ni, Fe, Co. Metal is volatized from ore using CO gas then decomposed to powder.
  • Atomisering: Used for Al, Mg, Ti alloys. Rapid solidification of molten metal forms powder upon gas or water atomization.
  • Vätgasreduktion: Used for W, Ta, Nb, Mo. Metal oxides heated in H2 gas causes oxygen removal leaving pure powders.
  • Plasmaatomisering: Used for reactive metals like Ti, Zr. Water interactions avoided by using plasma gas instead of water.
  • Smältning med elektronstråle: Used for Ti, Ta. High purity ingots levitated in vacuum melted by an electron beam then rapidly solidified by dropping through chamber.

High Purity Metal Powder Characteristics

ParameterDetaljerMätmetod
Fördelning av partikelstorlekVaries from 10 μm to 150 μmPartikelstorleksanalysator med laserdiffraktion
PartikelformSpherical, satellite, angular depending on production techniqueSEM-avbildning
TäthetCan approach theoretical density of the bulk materialPyknometri för gas
RenhetUp to 99.999% via strict process controls and handlingICP-OES kemisk analys
Impurity ElementsO, H, N, C most common contaminantsCombustion analysis followed by IR detection
FlödeskarakteristikEffects pourability, spreadability in AM machinesHall flowmeter funnel test

Applications of High Purity Metal Powders

IndustriTillämpningDesired Powder Attributes
Additiv tillverkning3D printing final partsControlled particle size distribution between 10-45 μm with good flow and packing is optimal
ElektronikConductive films, circuits, RF shieldingHigh purity above 99.9%, excellent conductivity, may require flake or dendritic powder
Welding WiresFörbättrad svetsstyrkaLow oxygen content below 100 ppm preferred
DiamantverktygCobalt binder increases tool lifespanHigh hardness, ability to take compressive loads without fracturing
MagnetsImproved residual inductionChemical compatibility with rare earth metals for sintering
Medicintekniska produkterKorrosionsbeständighet, biokompatibilitetPurity helps avoid metal ion leaching which may cause biological reactions

Benefits of High Purity Metal Powders

Using high purity metal powders enables:

  • More consistent chemistry and microstructure batch-to-batch
  • Achievement of electrical, magnetic, mechanical, and corrosion targets
  • Lower contamination risks
  • Attainment of strict aerospace and medical device standards
  • Improved product performance and lifespans
  • High value component production justifying increased powder cost
  • Design flexibility – customize alloy ratios and powder attributes as needed

Challenges With High Purity Metal Powders

DifficultyMitigating Actions
Högre kostnadPrioritize use only where function impacts justify premium price, minimize waste with stringent inventory controls
Limited Supply ChainPlan production schedules accounting for longer lead times, qualify multiple vendors
FuktkänslighetStore powder under vacuum or inert gases, requalify batches for degradation after shelf life expiration
Försiktighetsåtgärder vid hanteringEliminate iron contamination via use of non-magnetic tools, isolate from grinding or machining sources
ProcesstyrningPerform extensive parameter optimization, measurement, and documentation to ensure repeatability

metallpulver med hög renhet Prissättning

A cost comparison of Regular Grade vs High Purity nickel powder suitable for additive manufacturing is shown below:

ParameterRegular Nickel PowderHigh Purity Nickel Powder
Renhet98%-99% Ni>99.95% Ni
Syrehalt0.4%<0.01%
Kolinnehåll0.1%<0.02%
Sulfur Content0.01%<0.005%
Partikelstorlek15 to 45 μm15 to 45 μm
Kostnad per kg$50$240

Despite the higher cost, industries like aerospace rely exclusively on high purity powder even for prototype builds to prevent quality issues in final application.

metallpulver med hög renhet Leverantörer

Some leading suppliers offering high purity metal powders for industries like additive manufacturing include:

FöretagHeadquarters LocationErbjudna materialMarknader som betjänas
Sandvik OspreySverigeNi, Co, Cu, Al, Ti, moreAdditive manufacturing of end use components
AP&CKanadaTi, Ta, Nb Alloys, moreAerospace, medical, industrial
SnickeriteknikFörenta staternaNi, Co, moreConsumer electronics, aerospace
PraxairFörenta staternaTa, Nb, Mo alloysCapacitors, alloying agent
AMETEKFörenta staternaZr, Ti, W alloysMilitary, aerospace, semiconductor

metallpulver med hög renhet Kvalitetsstandarder

Key specifications relating to high purity metal powders include:

StandardOmfattningParameters Covered
ASTM B809Standard for annealed high purity Cu powder productionGoverns preparation method, chemical composition limits and impurities, particle size distribution, sampling
AMS-P-81748Ni powder used as additive manufacturing feedstockPurity, particle attributes, recommended handling and processing parameters
ASTM F3049Guide for characterizing properties of AM metal powdersTest procedures for powder morphology, flow rate, density, reuse guidelines
ASTM F3056Specification for additive manufacturing Ni alloy powderChemical composition, contamination limits, particle size distribution, lot sampling

These help ensure repeatable feedstock suited for demanding applications in aerospace, medical, electronics fields.

High Purity vs Regular Powders

ParameterPulver med hög renhetRegular Powder
RenhetUp to 99.999% pure98-99% range
SamstämmighetTightly controlled chemistry within 0.01%Can vary 1-3% batch-to-batch
PrestandaMeets strict industry standardsUnreliable, variable results
Pris4X to 10X higherLower cost per kg or pound
LedtidStock limitations, made to order in 10-12 weeks typicallyReadily available off the shelf
LeverantörskedjanSingle qualified vendorMultiple vendor options
TillämpningarAerospace, medical, nuclear, electronicsIndustrial prototypes, training builds

So while high purity powders carry a significant price premium, their unmatched consistency and standards conformance justify use in mission-critical applications where product performance directly correlates with powder quality.

metallpulver med hög renhet

Vanliga frågor

FrågaSvar
Why is high powder purity important for metal 3D printing or additive manufacturing?Impurities can alter local solidification rates leading to porosity or cracking that causes mechanical failure. Consistent chemistry and microstructure ensures repeatable material properties.
How are high purity levels achieved compared to conventional metal powders?Additional process steps like vacuum induction melting, atomization under inert gases, prevent atmospheric contamination during production. Handling under argon atmosphere avoids moisture or oxygen pickup.
Does high purity powder confer better corrosion resistance properties?Yes – contaminants often preferentially corrode leading to pitting. Reducing elements like sulfur, phosphorus, silicon to low ppm levels enhances corrosion resistance especially in acidic or saline environments.
Can you mix different purity level powders when printing a part?In general powders should not be mixed since the different chemistries may negatively interact. Exceptions could be blending small ratios of master alloy powders to adjust the matrix composition.

Sammanfattning

High purity metal powders with minimized oxygen, nitrogen and other impurities enable fabrication of components meeting strict aerospace, defense, medical, electronics and nuclear applications. Maintaining elemental chemistry control below 100 ppm ensures reliable electrical, mechanical, and corrosion performance. Common high purity metals include nickel, cobalt, aluminum alloys and refractory metals like tungsten or tantalum. While cost per unit mass is 4X to 10X higher than conventional powders, high purity materials are essential for mission-critical parts where product quality directly correlates with powder quality starting from raw material. With continual improvements in purity reaching beyond 99.999%, high purity metal powders will enable the next generation of components powering electric vehicles, spacecraft, satellites, and medical devices.

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MET3DP Technology Co, LTD är en ledande leverantör av lösningar för additiv tillverkning med huvudkontor i Qingdao, Kina. Vårt företag är specialiserat på 3D-utskriftsutrustning och högpresterande metallpulver för industriella tillämpningar.

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