Bästa IN939-pulver för 3D-utskrift 2024

IN939 pulver är en nickelbaserad superlegering som uppvisar exceptionella mekaniska egenskaper och hög motståndskraft mot korrosion och oxidation. Den består huvudsakligen av nickel, krom, kobolt, molybden och tantal. Denna sammansättning ger IN939-pulvret dess anmärkningsvärda styrka, värmebeständighet och stabilitet vid förhöjda temperaturer.

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Overview of IN939 Powder for 3D Printing

IN939 is a high-performance nickel-based superalloy powder designed for additive manufacturing of critical components needing exceptional mechanical properties at high temperatures. This article provides a comprehensive guide to IN939 powder for 3D printing applications across aerospace, automotive, energy and industrial sectors.

Key aspects covered include IN939 composition, properties, print parameters, applications, specifications, suppliers, handling, inspection, comparisons to alternatives, advantages and limitations, and frequently asked questions. Quantitative data is presented in easy-to-reference tables.

Composition of IN939 Powder

IN939 has a complex precipitation hardening alloy composition:

Element Vikt % Syfte
Nickel Balans Huvudmatriselement
Krom 15 – 18 Oxideringsbeständighet
Aluminium 3.8 – 4.8 Härdning genom utfällning
Titan 0.9 – 1.4 Härdning genom utfällning
Kobolt 12 – 15 Förstärkning av fast lösning
Tantalum 3.8 – 4.8 Hårdmetallformare
Kol 0.05 – 0.15 Hårdmetallformare
Bor 0.006 – 0.012 Grain boundary strengthener

Trace quantities of zirconium, magnesium and sulphur are also added for enhanced properties.

Properties of IN939 Powder

IN939 possesses an exceptional combination of properties:

Fastighet Beskrivning
Hög hållfasthet Excellent tensile and creep rupture strength up to 1050°C
Termisk stabilitet Strength maintained up to 1000°C
Krypbeständighet High stress-rupture life at high temperatures
Oxideringsbeständighet Forms protective Cr2O3 oxide scale
Motstånd mot termisk utmattning Resists cracking during thermal cycling
Fasstabilitet Microstructure stable after prolonged exposures
Korrosionsbeständighet Resistant to hot corrosion, oxidation, sulfidation

The properties enable use under extreme thermal and mechanical loads.

3D Printing Parameters for IN939 Powder

Typical AM processing parameters for IN939 include:

Parameter Typiskt värde Syfte
Skiktets tjocklek 20-50 μm Upplösning kontra bygghastighet
Laserkraft 250-500 W Tillräcklig smältning utan avdunstning
Skanningshastighet 800-1200 mm/s Density vs production rate
Avstånd mellan luckor 100-200 μm Mekaniska egenskaper
Stödstruktur Minimal Enkel borttagning
Varm isostatisk pressning 1160°C, 100 MPa, 3h Eliminerar porositet

Parameters are optimized for attributes like density, microstructure, build rate, and post-processing requirements.

Applications of 3D Printed IN939 Parts

Additively manufactured IN939 components serve critical applications including:

Industri Komponenter
Flyg- och rymdindustrin Turbine blades, vanes, combustors
Kraftproduktion Hot gas path parts, heat exchangers
Fordon Turbocharger wheels, valves
Kemisk bearbetning Pumpar, ventiler, reaktionskärl

Benefits over conventionally processed IN939 include complex geometries and reduced lead time.

Specifications of IN939 Powder for 3D Printing

IN939 powder for AM must meet exacting specifications:

Parameter Specifikation
Partikelstorlek 15-45 μm typiskt
Partikelns form Sfärisk morfologi
Skenbar densitet > 4 g/cc
Tappdensitet > 6 g/cc
Hall flödeshastighet > 23 sekunder för 50 g
Renhet >99,9%
Syrehalt <100 ppm

Tighter tolerances, custom size distributions, and controlled impurity levels available.

Suppliers of IN939 Powder

Reputable suppliers of IN939 powder include:

Leverantör Plats
Met3DP Kina
Snickare Tillsats USA
Praxair USA
AP&C Kanada
Erasteel Sverige
AMETEK USA

Pricing for IN939 powder ranges from $110/kg to over $220/kg based on quality and order volume.

Handling and Storage of IN939 Powder

As a reactive powder, careful handling of IN939 is needed:

  • Store sealed containers in a cool, inert atmosphere
  • Prevent contact with moisture, oxygen, acids
  • Använd korrekt jordad utrustning
  • Undvik ansamling av damm för att minimera explosionsrisken
  • Lokal avgasventilation rekommenderas
  • Wear appropriate PPE while handling

Proper techniques and controls prevent IN939 powder oxidation or contamination.

Inspection and Testing of IN939 Powder

IN939 powder is validated using:

Metod Testade parametrar
Analys av siktar Fördelning av partikelstorlek
SEM-avbildning Partikelns morfologi
EDX Kemi och sammansättning
XRD Befintliga faser
Pyknometri Täthet
Hall flödeshastighet Flödbarhet för pulver

Testing per applicable ASTM standards ensures batch consistency.

Comparing IN939 to Alternative Alloy Powders

IN939 compares to other Ni-based superalloys as:

Legering Hållfasthet vid höga temperaturer Kostnad Utskriftsmöjlighet Duktilitet
IN939 Utmärkt Hög Utmärkt Låg
IN738 Bra Medium Utmärkt Medium
IN718 Rättvist Låg Bra Utmärkt
Hastelloy X Utmärkt Hög Rättvist Medium

For balanced properties and processability, IN939 supersedes alternatives like IN718 Powder eller Hastelloy X Pulver.

Pros and Cons of IN939 Powder for 3D Printing

Proffs Nackdelar
Exceptional high temperature strength Expensive compared to IN718
Excellent oxidation and creep resistance Significant parameter optimization needed
Komplexa geometrier genomförbara Limited room temperature ductility
Faster processing than cast/wrought Controlled storage and handling environment
Comparable properties to cast alloy Svårt att bearbeta efter tryckning

IN939 enables high-performance printed parts but with higher costs and controlled processing needs.

Frequently Asked Questions about IN939 Powder for 3D Printing

Q: What particle size range works best for printing IN939?

A: A particle size range of 15-45 microns provides good flowability combined with high resolution and density. Finer particles below 10 microns can improve density and surface finish.

Q: Does IN939 require any post-processing after 3D printing?

A: Post processes like hot isostatic pressing, heat treatment, and machining are usually needed to eliminate porosity, relieve stresses, and achieve final tolerances and surface finish.

Q: What precision can be achieved with IN939 printed parts?

A: After post-processing, dimensional accuracy and surface finish comparable to CNC machined parts can be achieved with IN939 AM components.

Q: Are support structures necessary for printing IN939 powder?

A: Minimal supports are recommended for complex channels and overhangs to prevent deformation and facilitate easy removal. IN939 powder has good flowability.

Q: What alloy powder is the closest alternative to IN939 for AM?

A: IN738 is the closest alternative in terms of balanced properties and maturity for additive manufacturing. Other alloys like IN718 or Hastelloy X have some trade-offs.

Q: Is IN939 compatible with direct metal laser sintering (DMLS)?

A: Yes, IN939 is readily processable by major powder bed fusion techniques including DMLS along with selective laser melting (SLM) and electron beam melting (EBM).

Q: What density is achievable with 3D printed IN939 components?

A: With optimized parameters, densities over 99% are achievable, matching properties of traditionally processed IN939 products.

Q: How do the properties of printed IN939 compare to cast alloy?

A: Additively manufactured IN939 exhibits comparable or better mechanical properties and microstructure compared to conventional cast and wrought forms.

Q: What defects can occur when printing with IN939 powder?

A: Potential defects are cracking, distortion, porosity, surface roughness, incomplete fusion etc. Most can be prevented by proper parameter optimization and powder quality.

Q: Is hot isostatic pressing (HIP) mandatory for IN939 AM parts?

A: HIP eliminates internal voids and improves fatigue resistance. For less demanding applications, heat treatment alone may suffice instead of HIP.

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