Prášek ze slitiny niklu X750

Niklová slitina X750 je srážením kalitelná slitina niklu a chromu, která nabízí vynikající odolnost proti korozi a oxidaci. Vyznačuje se zachováním pevnosti, houževnatosti a tažnosti po kalení stárnutím a má pozoruhodnou pevnost při vysokých teplotách.

X750 má dobrou tvářitelnost v žíhaném stavu a lze jej snadno vyrobit pomocí standardních dílenských postupů tváření. Lze ji snadno kovat nebo jinak zpracovávat za tepla. Tváření za studena nepředstavuje žádné zvláštní problémy. Má také vynikající svařitelnost.

Zde je přehled vlastností a aplikací práškové slitiny niklu X750:

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Přehled

Prášek ze slitiny niklu X750 is a precipitation-hardenable nickel-chromium alloy that offers excellent resistance to corrosion and oxidation. It is noted for retaining strength, toughness and ductility after age hardening and has remarkable high temperature strength.

X750 má dobrou tvářitelnost v žíhaném stavu a lze jej snadno vyrobit pomocí standardních dílenských postupů tváření. Lze ji snadno kovat nebo jinak zpracovávat za tepla. Tváření za studena nepředstavuje žádné zvláštní problémy. Má také vynikající svařitelnost.

Zde je přehled vlastností a aplikací práškové slitiny niklu X750:

Složení:

  • Nickel: 70%
  • Chromium: 15%
  • Iron: 7%
  • Titanium and Aluminum additions

Vlastnosti:

  • Vynikající odolnost proti korozi a oxidaci
  • Retains high strength and toughness up to 1300°F (704°C)
  • Age hardenable
  • Easy to fabricate
  • Dobrá svařitelnost

Aplikace:

  • Gas turbines components
  • Součásti turbodmychadla
  • Heat treating fixtures
  • Nuclear fuel element spacers
  • Chemical and food processing equipment

Types and Designations

Nickel Alloy X750 powder is available with different particle size distributions:

Typ Velikost částic
Jemná třída 15-45 μm
Střední třída 45-106 μm
Hrubá třída 106-250 μm

It also has several standard specifications and designations:

  • UNS N07750
  • WNR 2.4668
  • AMS 5667
  • ASME SB-171
  • ASTM B640

Složení a vlastnosti

The typical composition and properties of Nickel Alloy X750 powder are:

Tabulka 1: Chemical composition of Nickel Alloy X750 powder

Živel Composition (%wt)
nikl (Ni) 70.0 min
Chrom (Cr) 14.0-17.0
železo (Fe) 5.0-9.0
titan (Ti) 0.7-1.2
hliník (Al) 0.2-1.0
uhlík (C) 0,08 max.
mangan (Mn) 1,0 max
křemík (Si) 1,0 max
měď (Cu) 0,5 max.
síra (S) 0,015 max
fosfor (P) 0,015 max

Tabulka 2: Physical properties of Nickel Alloy X750 powder

Vlastnictví Hodnota
Hustota 8.36 g/cc
Bod tání 2400-2550°F (1315-1399°C)
Tepelná vodivost 9.4-12.4 W/m-K (68-218°F)
Modul pružnosti 31 x 106 psi
Elektrický odpor 617 μΩ-cm
Koeficient tepelné roztažnosti 8.1 x 10-6/°F (14.6 μm/m-°C)

Tabulka 3: Mechanical properties of Nickel Alloy X750 powder

Mechanické vlastnosti Hodnota
Pevnost v tahu 190-240 ksi (1310-1655 MPa)
0.2% Yield Strength 140-190 ksi (965-1310 MPa)
Prodloužení 10-22%
Tvrdost Rockwell C 35-45

Aplikace a použití

Some of the key applications for Nickel Alloy X750 powder include:

Tabulka 4: Applications of Nickel Alloy X750 powder

Průmysl Aplikace
Aerospace Gas turbine engine components, Turbocharger components
Automobilový průmysl Exhaust valves and components
Průmyslový Heat treating fixtures and trays
Ropa a plyn Wellhead components, valves, pumps
Chemické Reactor vessels, piping, heat exchangers
Zpracování potravin Pressure vessels, evaporators
Jaderné Fuel element spacers and springs

The excellent heat and corrosion resistance make X750 suitable for use in high temperature environments seen in gas turbines, turbochargers, industrial furnaces and other extreme applications up to 1300°F (704°C).

Its high strength is valuable for components under mechanical stresses like valves, pumps and high pressure vessels and piping.

The outstanding room temperature tensile, yield, and creep-rupture properties in combination with oxidation resistance and fabricability provide proven advantages for many critical chemical processing industry applications.

Specifikace a dostupnost

Nickel Alloy X750 powder is readily available from leading global specialty metal suppliers in various size distributions:

Tabulka 5: Nickel Alloy X750 powder sizes and dimensions

Typ Velikost částic **ASTM Screen Size **
Ultrafine 1-5 μm N/A
Pokuta 15-45 μm -325 ok
Střední 45-106 μm 140-325 ok
Hrubý 106-250 μm -140 mesh

Tabulka 6: Indicative pricing for Nickel Alloy X750 powder

Typ Stav Cena ($/kg)
Prášek -325 ok $75 – $150
Prášek 140-325 Mesh $50 – $120
Prášek -140 ok $45- $100

Pricing can vary based on quantity and exact specifications. Contact leading manufacturers and suppliers for custom quotes.

Comparison with Alloy 718

Nickel Alloy X750 is part of the high-performance nickel-chromium family with similar compositions to the popular Alloy 718.

Here is a comparison between Alloy X750 and Alloy 718 powders on key parameters:

Tabulka 8: Nickel Alloy X750 vs. Alloy 718 Comparison

Vlastnictví X750 718
Hustota (g/cc) 8.36 8.19
Melting Range (°F) 2400-2550 2300-2350
Pevnost v tahu (ksi) 190-240 160-220
Pevnost v tahu Lepší Dobrý
Zpracovatelnost Lepší Mírný
Svařitelnost Vynikající Mírný
Odolnost proti korozi Vynikající Mírný
Odolnost proti oxidaci Vynikající Špatný
Náklady Mírný Inexpensive
Dostupnost Mírný Readily Available

In summary, Alloy X750 demonstrates:

  • Higher creep strength for high temperature serviceability
  • Better fabricability and weldability for ease of manufacture
  • Significantly improved corrosion and oxidation resistance
  • Moderate cost premium over 718

Alloy X750 is the preferred choice for extreme environments while Alloy 718 offers a more economical solution for less critical applications.

Výhody a omezení

Some of the main advantages and limitations of Nickel Alloy X750 powder include:

Tabulka 9: Advantages of Nickel Alloy X750 powder

Výhody
Excellent room temperature tensile, yield and rupture strength
Retains tensile strength up to 1300°F (704°C)
Resistant to creep and thermal fatigue cracking
Outstanding resistance to corrosion in reducing and oxidizing media up to 1800°F (982°C)
Excellent oxidation resistance up to 2200°F (1204°C)
Good formability in annealed state
Readily forged or hot worked
Easy to weld using conventional methods

Processing and Manufacturing

Nickel Alloy X750 powder can be processed into finished components using various methods:

Casting

  • Investment casting is commonly used. Ceramic molds enable pouring at 2600-2800°F (1427-1538°C). Produces highly sound castings.
  • Sand casting can also be done but extra feeding of liquid metal is needed to get soundness. Special sand binders may be required.
  • Shell mold casting yields products comparable to investment cast. Thin rolls can be produced.
  • Continuous casting in graphite molds is widely used for producing billets for further processing.

Table 11: Casting specifications

Proces Velikosti Tolerance Finishes
Investment 0.1-100 lbs ± 0.030 in/in As-cast, HIP
Sand 25-2000 lbs ± 0.125 in/in As-cast, ground
Shell 0.5-75 lbs ± 0.060 in/in As-cast
Continuous Cast 3-12 in dia billets ± 0.125 in/in dia Hot worked

Typical casting defects like hot tears, microporosity and segregation can occur but can be minimized by proper gating/risering, mold design and pouring/shakeout practices.

Deformation Processing

Hot working is performed between 2150-2300°F (1177-1260°C) followed by air cooling. Warm working is done below 1900°F (1038°C). Cold working may require intermediate annealing.

Common methods include:

  • Forging: Closed die process produces best properties
  • Rolling: Both flat and shape rolling performed. Minimum thickness reduction 30%
  • Extrusion: Excellent properties achieved in sections up to 8 in dia
  • Drawing: Heavy wire/bar can be drawn. Intermediate softening may be needed.

Table 12: Key specifications

Metoda Size ranges Reductions Finishes
Kování 0.1-1000 lbs 30-90% Hot worked
Rolling 0.05-500 lbs 30-80% Hot band
Vytlačování 0.5-500 lbs 75-90% As extruded
Drawing 0.003-3 in dia 30-65% Bright annealed

Joining Processes

All standard methods can effectively join X750 parts. Matching alloys preferred for optimum properties.

Svařování: Gas tungsten arc (GTAW) and gas metal arc welding (GMAW) most widely employed. Resistance and laser beam welding also occasionally applied. Matching composition filler rods are used. Joints exhibit excellent strength. Proper preheat and post weld heat treatment essential to avoid cracking.

Pájení: Vacuum brazing gives best combination of strength and temperature resistance. Various silver braze alloys used with brazing done at 1900-2000°F (1038-1093°C). Critical to control clearances, fluxes and atmosphere.

Table 13: Joining recommendations

Proces Metody Filler Metals Komentáře
Svařování GTAW, GMAW Alloy 625, 725 Observe maximum interpass temps
Pájení Vakuum Silver brazes Fluxless preferred
Cladding Roll bonding Slitiny mědi Hot roll plated
Fastening Bolting, riveting Alloy X750 Use cold worked holes

Post Processing Treatments

Solution heat treating and age hardening are used to develop optimum properties:

Řešení Ošetření – Performed at 2100-2300°F (1149-1260°C) followed by air or water quenching. Enables subsequent age hardening.

Age Hardening – Age at 1325-1425°F (± 25°F) for 10-50 hours followed by air cooling. Achieves precipitation hardening for maximum strength levels.

Optional stabilization treatment involves 850-1200°F for 1-16 hours to stabilize against future property changes.

Table 14: Post processing specifications

Proces Léčba Expected Properties
Solution Treating 2150°F (1177°C), 30 min, AC Optimized microstructure
Age Hardening 1350°F (732°C), 24 hrs, AC 190-240 ksi UTS
Stabilization 1000°F (538°C), 4 hrs, AC Stable hardness

Powder Production

Nickel Alloy X750 powder is commercially produced by gas atomization and water atomization methods. Particle size distribution tightly controlled through specialized nozzles and calibrated sieving. High purity inert gas used to prevent contamination.

Table 15: Powder production methods

Proces Velikosti Rate Čistota
Atomizace plynu 10-250 μm 30-200 kg/hr 99.9%
Atomizace vody 25-150 μm 20-100 kg/hr 99.7%

Both gas and water atomized powders show spherical particle morphology ideal for additive manufacturing, metal injection molding and other powder metallurgy applications.

Design Data

Key design data parameters for Nickel Alloy X750 are summarized below for reference during engineering and component design activities:

Table 16: Design data parameters for Nickel Alloy X750

Kategorie Hodnoty Komentáře
Hustota 0.302 lb/in3 Moderate weight
Youngův modul 30.8 x 106 psi Tuhost
Poissonův poměr 0.294
Modul ve smyku 11.7 x 106 psi Resistance to shape change
Elektrický odpor 617 μΩ-cm Higher resistance than copper
Koeficient tření 0.46-0.80 Varies based on surface finish
Tepelná vodivost 113-124 BTU-in/hr-ft2-°F Higher than stainless steels
Měrné teplo 0.106 BTU/lb-°F
Mean CTE 7.3 x 10-6 in/in-°F Average between RT-500°F
Prandtl Number 0.012 Ratio of momentum diffusivity to thermal diffusivity
Heat Transfer Coefficient 120-200 BTU/hr-ft2-°F Depends on environment

Structural Load Conditions

For structural engineering calculations at temperature extremes, use:

  • Tensile yield strength: 140-190 ksi
  • Compressive yield strength: 170-220 ksi
  • Modular ratio, E (Alloy X750)/E (Steel): 1.0

At room temperature up to 500°F – Moderate corrosion rate of less than 0.002 in/yr expected.

Up to 1900°F – Excellent resistance to hot corrosion and oxidation. Use parabolic rate constant kp = 3.4 x 10-8 mg2/cm4/s.

Odolnost proti tečení a únavě

Alloy X750 demonstrates excellent creep resistance. Rupture strength higher than 80 ksi for 100,000 hrs at 1300°F (980°C).

For cyclic fatigue conditions, use:

  • Endurance (106 cycle) fatigue strength of 95-100 ksi
  • Reduction factor of 1.0 for machined surface finish rather than as-fabricated

Environment has small effect on fatigue strength. Use fatigue reduction factor = 0.95 for air environment.

Machining Nickel Alloy X750

Nickel Alloy X750 has excellent machinability in the annealed state and can be machined using most standard workshop methods and tools.

Chip breakers recommended for effective chip control. Rigid setups needed to minimize vibration. Positive rake cutting tools with sharp cutting edges provide longest tool life.

Low thermal conductivity leads to heat concentration so copious coolant should be used.

Table 17: Machining methods

Metoda Tool Materials Speeds/Feeds Komentáře
Otáčení High speed steel, Carbide, Ceramic, CBN, PCD 100-250 sfm Use heavy depths of cut
Vrtání Carbide with TiAlN coating 10-30 sfm Peck drill larger diameters
Threading Carbide inserts 4-10 ipr Maintain tool nose radius
Frézování Carbide,

Processing and Manufacturing

Nickel Alloy X750 powder can be processed into parts using various methods:

Aditivní výroba

Additive manufacturing (AM), also known as 3D printing, uses the nickel alloy powder as feedstock for building up components layer by layer. Some AM techniques suitable for X750 include:

Přímé laserové spékání kovů (DMLS)

  • Powder is selectively melted by a high power laser
  • Produces fully dense parts with fine microstructure
  • Vynikající rozměrová přesnost a kvalita povrchu
  • Možnost použití složitých geometrií

Tavení elektronovým paprskem (EBM)

  • Powder is melted by an electron beam in vacuum
  • Achieves near full density with good strength
  • Lower surface finish compared to laser processes
  • Fast build rates due to higher beam power

Tryskání pojiva

  • Liquid bonding agent selectively deposited to join powder particles
  • Cost-effective process with high productivity
  • Requires post-processing like sintering and infiltration
  • Larger parts possible with good geometric freedom

Cold Spray

  • Powder particles accelerated to supersonic speeds and impacted on to a substrate
  • Kinetic energy bonds particles to surface
  • Thick coatings and freeform shapes can be built up
  • Minimal heating preserves base material properties

Table 11: Additive manufacturing processes for Nickel Alloy X750

Proces Přesnost Povrchová úprava Mechanické vlastnosti Geometrie Rychlost
DMLS Vysoký Vynikající Predictable Komplexní Pomalý
EBM Vysoký Mírný Consistent Komplexní Mírný
Binder jet Mírný Špatný Variabilní Jednoduché Rychle
Studený sprej Nízký Hrubý Anizotropní Jednoduché Rychle

Parameters like laser power, beam size, hatch spacing, and scanning strategy can be optimized to control part density, surface quality, microstructure and mechanical performance.

Heat treatments like hot isostatic pressing (HIP) and aging may be applied post-processing to further enhance densification and material properties.

Casting

The X750 alloy can also be induction melted and cast into ingots, billets and bars using processes like:

  • Vakuové indukční tavení
  • Electroslag remelting
  • Investiční lití

Cast products serve as feedstock for subsequent breakdown operations like forging, rolling and extrusion. They can also be machined directly into net shape components.

Deformation Processing

Various deformation techniques can be applied to cast nickel alloy feedstock:

Kování

  • Pressing or hammering cast ingots between dies
  • Improves strength through grain flow and work hardening
  • Near net shapes can be achieved

Rolling

  • Compressing and reducing thickness between rolls
  • Produces sheets, strips and plates
  • Controls grain structure and enhances properties

Vytlačování

  • Forcing through a die opening
  • Forms long sections with fixed cross-section
  • Dense product with uniform fine grains

Drawing

  • Pulling through a die using tensile force
  • Reduces cross-section of bars, tubes or wires
  • Zvýšená pevnost a tvrdost

The alloy is annealed periodically during working to restore ductility and avoid cracking. Final heat treatment and aging follows to achieve desired characteristics.

Nejčastější dotazy

Q: What is Nickel Alloy X750?

A: X750 is a precipitation-hardenable nickel-chromium alloy with excellent strength up to 1300°F (700°C), outstanding corrosion and oxidation resistance, and good fabrication characteristics.

Q: What are the typical applications for X750?

A: Gas turbines components, turbocharger parts, nuclear fuel elements, chemical processing equipment, food processing vessels – anywhere needing capability at high temperatures in harsh environments.

Q: Is Nickel Alloy X750 weldable?

A: Yes, X750 has good weldability for a high-strength precipitation-hardened alloy. Gas tungsten arc and gas metal arc welding can produce sound welds. Stress relieving heat treatment is often employed after welding.

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